No Moss 3 Landfill Online Library Gentry Locke 2024-06-14-Gentry Locke FOIA 23-1479 - Bloated Material- Russel County Reclamations - ASTM C330 Verification Testing - 2-6-2024

23-1479 - Bloated Material- Russel County Reclamations - ASTM C330 Verification Testing - 2-6-2024

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February 6, 2024

Mr. John Matney

Russell County Reclamation LLC Phone: 423-646-3400 2389 Lee Hwy E-mail: [email protected] Bristol, VA 24201

Subject: Final Report of ASTM C 330-17a

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Mr. Matney

SGS TEC Services is an AASHTO R18, ANS/ISO/IEC 17025:2017, and is an Army Corps of Engineers

accredited laboratory. SGS TEC Services is pleased to present this interim report of our testing on the

expanded lightweight aggregate submitted to our laboratory in August of 2023. The results of this testing

pertain only to the samples tested. The aggregate was tested in accordance with the applicable sections of

ASTM C330-17 Standard Specification for Lightweight Aggregates for Structural Concrete.

This specification covers lightweight aggregates intended for use in structural concrete in which prime

considerations are reducing the density while maintaining the compressive strength of the concrete. The

maximum and minimum requirements for this specification are presented in Section 5 Chemical

Composition and Section 6 Physical Properties of ASTM C330 and are reported in Table 1. Based on our

results to date, the 1/2 Structural lightweight aggregate labeled as Bloated Material (Russell County

Reclamation) submitted to our laboratory meet and/or exceeds the requirements of ASTM C330.

TEC SERVICES

Testing * Engineering * Consulting

February 6, 2024

Mr. John Matney

Russell County Reclamation LLC Phone: 423-646-3400 2389 Lee Hwy E-mail: [email protected]

Bristol, VA 24201

Subject: Final Report of ASTM C 330-17 Bloated Material - Russell County Reclamation SGS TEC Services Sample ID: 23-1479

Mr. Matney

SGS TEC Services is an AASHTO R18, ANS/ISO/IEC 17025:2017, and is an Army Corps of Engineers accredited laboratory. SGS TEC Services is pleased to present this interim report of our testing on the expanded lightweight aggregate submitted to our laboratory in August of 2023. The results of this testing pertain only to the samples tested. The aggregate was tested in accordance with the applicable sections of ASTM C330-17 Standard Specification for Lightweight Aggregates for Structural Conerete.

This specification covers lightweight aggregates intended for use in structural concrete in which prime considerations are reducing the density while maintaining the compressive strength of the conerete. The maximum and minimum requirements for this specification are presented in Section 5 Chemical Composition and Section 6 Physical Properties of ASTM C330 and are reported in Table 1. Based on our results to date, the 1/2 Structural lightweight aggregate labeled as Bloated Material (Russell County Reclamation) submitted to our laboratory meet and/or exceeds the requirements of ASTM C330.

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bk 770-995-8000 | www.tecservices.com os

Final Report of ASTM C 330-17a February 6, 2024

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Page 2 of 8

Table 1: Summary of Test Results

Section 5 - Chemical Composition Test Results ASTM C330

Requirements

Organic Impurities (Color change) < 1 3 (max)

Staining (Stain index) 0 60 (max)

Loss on Ignition 2.33 5% (max)

Section 6 – Physical Properties

Clay Lumps and Friable Particles (Dry mass) 0.3 % 2% (max)

Bulk Density (Loose) 47 lb/ft3 55 lb/ft3 (max)

Relative Density (Specific Gravity) (Saturated Surface-dry) 1.634 ----

Relative Density (Specific Gravity) (Oven-Dry) 1.500 ----

72-Hour Absorption 8.93 % ----

Compressive Strength

(Requirement based off Calculated Equilibrium Density) 4380 3,740 psi (min)

Splitting Tensile

(Requirement based off Calculated Equilibrium Density) 440 325 psi (min)

Drying Shrinkage -0.032 -0.070 % (max)

Popouts No Popouts No Popouts

Grading See Grading Below

Resistance to Freezing and Thawing (Relative Dynamic Modulus, %) 100 ----

Organic Impurities

The organic impurities were tested in accordance with ASTM C40-20 Standard Test Method for Organic

Impurities in Fine Aggregates for Concrete.

Requirement – Lightweight aggregate subjected to the test for organic impurities shall not produce darker

color than standard.

Result – The lightweight aggregate did not show any color change.

Iron Staining

The staining testing was tested in accordance with ASTM C641-17 Standard Test Method for Iron

Staining Materials in Lightweight Concrete Aggregates.

Requirement – Lightweight aggregate shall have a stain index of less than sixty.

Result – The lightweight aggregate showed no stain, which indicates an index of 0.

Loss on Ignition

Final Report of ASTM C330-17a Bloated Material - Russell County Reclamation SGS TEC Services Sample ID: 23-1479

Table 1: Summary of Test Results

February 6, 2024

Section 5 - Chemical Composition Test Resutts | ASTM C330 Requirements ‘Organic Impurities (Color change) <1 3 (max) Staining (Stain index) 0 60 (max) Loss on Ignition 233 5% (max) Section 6 — Physical Properties

Clay Lumps and Friable Particles (Dry mass) 03% % (max) Bulk Density (Loose) 7b | 55 TDA (max) Relative Density (Specific Gravity) (Saturated Surface-dry) 1.634 = Relative Density (Specific Gravity) (Oven-Dry) 1.500 72-Hour Absorption 893% ‘Compressive Strength ami (Requirement aed off Calculated Equilibrium Density) 4380 3.740 psi (min) Splitiing Tensile (Requirement based off Calculated Equilibrium Density) 440 325 psi (min) Drying Shrinkage 0.032 | -0.070 % (max) Popouts No Popouts | No Popouts Grading See Grading Below

Resistance to Freezing and Thawing (Relative Dynamic Modulus, %)

100

Organic Impurities

The organic impurities were tested in accordance with ASTM C40-20 Standard Test Method for Organic

Impurities in Fine Aggregates for Concrete

Requirement ~ Lightweight aggregate subjected to the test for organic impurities shall not produce darker

color than standard.

Result ~ The lightweight aggregate did not show any color change.

Iron Staining

The staining testing was tested in accordance with ASTM C641-17 Standard Test Method for Iron

Staining Materials in Lightweight Concrete Aggregates.

Requirement — Lightweight aggregate shall have a stain index of less than sixty.

Result — The lightweight aggregate showed no stain, which indicates an index of 0.

Loss on Ignition

Page 2 of 8

Final Report of ASTM C 330-17a February 6, 2024

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Page 3 of 8

The loss of ignition was tested in accordance with ASTM C114-18 Standard Test Methods for Chemical

Analysis of Hydraulic Cement.

Requirement – Lightweight aggregate shall have a loss of ignition not more than five percent.

Result – The material had a loss on ignition percentage of 2.33.

Clay Lumps and Friable Particles

The clay lumps and friable particles was tested in accordance with ASTM C142-17 Standard Test Method

for Clay Lumps and Friable Particles in Aggregates.

Requirement – The amount of clay lumps and friable particles shall not exceed two percent by

dry mass.

Results – The lightweight aggregate had 0.3 percent clay lumps and friable aggregate.

Grading

The grading was tested in accordance with ASTM C136-19 Standard Test Method for Sieve Analysis of

Fine and Coarse Aggregates. The grading shall conform to the requirements in Table 1 of ASTM C330.

The Grading and the required grading are reported in Table 2.

Table 2: Grading & Required Grading

Sieve Size % Passing Required % Passing

(1/2 to #4)

¾ in 100.0 100

½ in 93.2 90 - 100

3/8 in 62.0 40 - 80

#4 13.8 0 - 20

#8 5.8 0 - 10

#16 3.5 —

#50 1.5 —

#100 0.7 —

#200 0.3 0 - 10

NOTE: The received material was crushed in a jaw-type crusher at SGS TEC Services in order to achieve

the grading listed above.

Final Report of ASTM C 330-174 February 6, 2024 Bloated Material - Russell County Reclamation SGS TEC Services Sample ID: 23-1479

The loss of ignition was tested in accordance with ASTM C1 14-18 Standard Test Methods for Chemical Analysis of Hydraulic Cement.

Requirement — Lightweight aggregate shall have a loss of ignition not more than five percent. Result — The material had a loss on ignition percentage of 2.33.

Clay Lumps and Friable Particles ‘The clay lumps and friable particles was tested in accordance with ASTM C142-17 Standard Test Method

for Clay Lumps and Friable Particles in Aggregates.

Requirement ~ The amount of clay lumps and friable particles shall not exceed two percent by dry mass. Results ~ The lightweight aggregate had 0.3 percent clay lumps and friable aggregate.

Grading The grading was tested in accordance with ASTM C136-19 Standard Test Method for Sieve Analysis of Fine and Coarse Aggregates. The grading shall conform to the requirements in Table 1 of ASTM C330.

The Grading and the required grading are reported in Table 2.

Table 2: Grading & Required Grading

Sieve Size oh Passing Required % Passing (1/2 to #4) Yin 100.0 700 ’in 93.2 90 - 100 “in 62.0 40-80 #4 13.8 0-20 #8 5.8 0-10 #16 35 = #50 15 = #100 07 = #200 03 0-10

NOTE: The received material was crushed in a jaw-lype crusher at SGS TEC Services in order to achieve the grading listed above.

Page 3 of &

Final Report of ASTM C 330-17a February 6, 2024

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Page 4 of 8

Bulk Density (Loose)

The oven dried loose bulk density was tested in accordance with Method C-Shoveling of ASTM C29-17a

Standard Test Method for Bulk Density (“Unit Weight”) and Voids in Aggregate.

Requirement – The maximum bulk density (loose) for coarse aggregate is 55 lbs/ft3.

Result – The lightweight aggregate had an average bulk density (loose) of 47 lb/ft3.

Specific Gravity & Absorption

The relative density and absorption were tested in accordance with ASTM C127-15 Standard Test

Method for Density, Relative Density (Specific Gravity) & Absorption of Coarse Aggregate. The sample

was dried to a constant mass and soaked for 72 hours. The specific gravity and absorption are reported in

Table 3.

Table 3: Specific Gravity & Absorption

Absorption after 72-hour Soak

(percent)

Relative Density

(Specific Gravity)

(Oven-Dry)

Relative Density

(Specific Gravity)

(Saturated Surface-Dry)

8.93 1.500 1.634

Concrete mixtures containing the lightweight aggregate were batched to make test specimens for

compressive strength, splitting tensile, drying shrinkage and resistance to freezing and thawing. The

material sources and amount of material used in the concrete mix are reported in Table 4. Fresh

properties are reported in Table 5.

Table 4: Mix Proportions

Material Source Amount

(pcy)

Portland Type I/II Cement Cemex - Clinchfield 564

Fine Aggregate – Natural Sand Lambert, Wiregrass 1450

Lightweight Aggregate – (1/2” to #4) Russel County Reclamation 940

Air Entrainment Vinsol Resin 1.2 oz/yd³

Water Reducer Type F – High Range 4.0 oz/yd³

Water Lawrenceville City Water 278

Total 3,232

Final Report of ASTM C 330-17a February 6, 2024 Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Bulk Density (Loose) The oven dried loose bulk density was tested in accordance with Method C-Shoveling of ASTM C29-17a Standard Test Method for Bulk Density (“Unit Weight”) and Voids in Aggregate.

Requirement — The maximum bulk density (loose) for coarse aggregate is 55 Ibs/ft’. Result ~ The lightweight aggregate had an average bulk density (loose) of 47 Ib/ft

Specific Gravity & Absorption The relative density and absorption were tested in accordance with ASTM C127-15 Standard Test

Method for Density, Relative Density (Specific Gravity) & Absorption of Coarse Aggregate. The sample ‘was dried to a constant mass and soaked for 72 hours. The specific gravity and absorption are reported in Table 3

Table 3: Specific Gravity & Absorption

Absorption after 72-hour Soak (percent)

Relative Density (Specific Gravity) (Oven-Dry)

Relative Density (Specific Gravity) (Saturated Surface-Dry)

8.93

1,500

1.634

Concrete mixtures containing the lightweight aggregate were batched to make test specimens for compressive strength, splitting tensile, drying shrinkage and resistance to freezing and thawing. The material sources and amount of material used in the concrete mix are reported in Table 4, Fresh

properties are reported in Table 5.

‘Table 4: Mix Proportions

Material Source Amount (pey) Portland Type Will Cement Cemex - Clinchfield 564 Fine Aggregate ~ Natural Sand Lambert, Wiregrass 1450 Lightweight Aggregate ~(1/2 to #4) _| Russel County Reclamation 940 ‘Air Entrainment Vinsol Resin T2ozye Waiter Reducer Type F— High Range 40 oziye Water Lawrenceville City Water 278 Total 3.232

Page 4 of &

Final Report of ASTM C 330-17a February 6, 2024

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Page 5 of 8

Table 5: Fresh Properties

Slump (inches) 2.25

Unit Weight (lb/ft3) 119.4

Air Content (%) 6.0

Concrete Temperature (°F) 73

The oven-dry density of the concrete mixture was calculated by the mixture quantities, aggregate

moisture content, and the volume of the concrete batch. The calculated equilibrium density of 113.7 lb/ft³

was calculated by adding 3 lb/ft³ to the calculated oven-dry density. The calculated equilibrium density is

used to determine the specification requirements for the compressive and split tensile strengths.

Compressive Strength and Splitting Tensile Strength

Compressive Strength

The compressive strength was tested in accordance with ASTM C39-21 Standard Test Method for

Compressive Strength of Cylindrical Concrete Specimens.

Requirement – For concrete with combinations of normal weight and lightweight aggregates and a

calculated equilibrium density of 113.7 lb/ft3, the minimum compressive strength is 3,740 psi. This was

calculated by interpolation from the values presented in section 5.2.1 and are reported in Table 6. The

specimens tested were 4” x 8” cylinders and the results are reported in Table 7.

Table 6: Compressive & Splitting Tensile Strength Requirements

Calculated Equilibrium Density

(lbs/ft3)

Splitting Tensile Strength

Requirements (psi)

Compressive Strength

Requirements

(psi)

110 310 3,000

115 330 4,000

Final Report of ASTM C 330-17a February 6, 2024 Bloated Material - Russell County Reclamation SGS TEC Services Sample ID: 23-1479

Table 5: Fresh Properties

‘Slump (inches) 2.25

Unit Weight (Ib/f*) 119.4 Air Content (%) 60 Conerete Temperature °F) 7B

The oven-dry density of the concrete mixture was calculated by the mixture quantities, aggregate moisture content, and the volume of the conerete batch. The calculated equilibrium density of 113.7 Ib/ft? was calculated by adding 3 Ib/ft to the calculated oven-dry density. The calculated equilibrium density is used to determine the specification requirements for the compressive and split tensile strengths,

Compressive Strength and S|

Strength

Compr The compressive strength was tested in accordance with ASTM C39-21 Standard Test Method for Compressive Strength of Cylindrical Concrete Specimens

Requirement — For concrete with combinations of normal weight and lightweight aggregates and a calculated equilibrium density of 113.7 Ib/ft, the minimum compressive strength is 3,740 psi. This was calculated by interpolation from the values presented in section 5.2.1 and are reported in Table 6. The specimens tested were 4” x 8” cylinders and the results are reported in Table 7.

Table 6: Compressive & Splitting Tensile Strength Requirements

  • 7" ; ‘Compressive Strength Calculated Equilibrium Density Splitting Tensile Strength i" rt’) A . Requirements (bsift’) Requirements (psi) i

(psi)

110 310 3,000

115 330 4,000

Page 5 of 8

Final Report of ASTM C 330-17a February 6, 2024

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Page 6 of 8

Table 7: Compressive Strength Results

Sample ID Compressive Strength

(psi)

23-1479-A 4,200

23-1479-B 4,540

23-1479-C 4,600

23-1479-D 4,190

Average 4,380

Splitting Tensile

The splitting tensile strength was tested in accordance with C496 C496M-17 Standard Test Method for

Splitting Tensile Strength of Cylindrical Concrete Specimens.

Requirement – For a concrete with combinations of normal weight and lightweight aggregates and a

calculated equilibrium density of 113.7 lb/ft3, the minimum splitting tensile strength is 325 psi. The

specimens tested were 6” x 12” cylinders and the results are reported in Table 8.

Table 8: Splitting Tensile Strength Result

Sample ID Splitting Tensile Strength (psi)

23-1479-1 520

23-1479-2 385

23-1479-3 510

23-1479-4 480

23-1479-5 445

23-1479-6 395

23-1479-7 400

23-1479-8 390

Average 440

Drying Shrinkage

The drying shrinkage testing was tested in accordance with C157-17 Standard Test Method for Length

Change of Hardened Hydraulic-Cement Mortar and Concrete and modified per ASTM C330. Three

length change beams (4” x 4” x 11¼”) were moist cured for seven days. Upon the completion of the 7-

day moist curing an initial reading was obtained, which was used as the base length for the drying

shrinkage calculations. The samples were then placed in a curing cabinet maintained at 100 ± 2°F with a

relative humidity of 32 ± 2% for 28 days.

Requirement – The drying shrinkage of the concrete specimens shall not exceed 0.07% at 28days.

Final Report of ASTM C 330-174 February 6, 2024 Bloated Material - Russell County Reclamation SGS TEC Services Sample ID: 23-1479

Table 7: Compressive Strength Results

Sample 1D Compressive Strength (psi) 23-1479-A 4,200 23-1479-B 4540 23-1479-C 4,600 23-1479-D 4,190 ‘Average 4,380

Splitting Tensile

The splitting tensile strength was tested in accordance with C496 C496M-17 Standard Test Method for Splitting Tensile Strength of Cylindrical Concrete Specimens

Requirement ~ For a conerete with combinations of normal weight and lightweight aggregates and a calculated equilibrium density of 113.7 Ib/ft’, the minimum splitting tensile strength is 325 psi. The specimens tested were 6” x 12” cylinders and the results are reported in Table 8.

Table 8: Splitting Tensile Strength Result

Sample ID Splitting Tensile Strength (psi) 23-1479-1 520 23-1479-2 385 23-1479-3 310 23-1479-4 480 23-1479-5 445 23-1479-6 395 23-1479-7 400 23-1479-8 390 ‘Average 440

Drying Shrinkage

The drying shrinkage testing was tested in accordance with C1S7-17 Standard Test Method for Length Change of Hardened Hydraulic-Cement Mortar and Concrete and modified per ASTM C330. Three length change beams (4” x 4” x 11%”) were moist cured for seven days. Upon the completion of the 7- day moist curing an initial reading was obtained, which was used as the base length for the drying shrinkage calculations. The samples were then placed in a curing cabinet maintained at 100 + 2°F with a relative humidity of 32 + 2% for 28 days.

Requirement ~ The drying shrinkage of the concrete specimens shall not exceed 0.07% at 28days

Page 6 of 8

Final Report of ASTM C 330-17a February 6, 2024

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Page 7 of 8

Table 9: Drying Shrinkage at 28 Days

Sample ID Length Change at 28 Days

(%) 23-1479 (1) -0.033

23-1479 (2) -0.032

23-1479 (3) -0.032

Average -0.032

Popouts

Requirement – There shall be no popouts observed after test concrete made with the tested lightweight

aggregate is subjected to an autoclave in accordance with ASTM C151-18 Standard Test Method for

Autoclave Expansion of Hydraulic Cement.

Result – No popouts were observed.

Resistance to Freezing and Thawing

The freeze-thaw samples were tested in accordance with ASTM C666-15 Resistance of

Concrete to Rapid Freezing and Thawing – Procedure A (freezing and thawing in water) with

the curing modifications listed in ASTM C330.

Results – The average relative dynamic modulus after 300 cycles was 100%.

Results are reported in Table 10.

Table 10– Freeze-Thaw Testing – Cast Concrete Samples (3 beams)

Final Report of ASTM C330-17a

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-147

9

February 6, 2024

Table 9: Drying Shrinkage at 28 Days

Sample ID Tength Change at 28 Days (%) 23-1479 (1) 0,033 23-1479 (2) 0.032 23-1479 (3) 0.032 Average 0.032

Popouts

Requirement ~ There shall be no popouts observed after test concrete made with the tested lightweight aggregate is subjected to an autoclave in accordance with ASTM C151-18 Standard Test Method for

Autoclave Expansion of Hydraulic

Cement.

Result ~ No popouts were observed.

Resistance to Freezing and Thawing The freeze-thaw samples were tested in accordance with ASTM C666-15 Resistance of

Concrete to Rapid Freezing and Thawing ~ Procedure A (freezing and thawing in water) with

the curing modifications listed i

in ASTM €330,

Results ~ The average relative dynamic modulus after 300 cycles was 100%.

Results are reported in Table 10.

Table 10— Freeze-Thaw Testing — Cast Concrete Samples (3 beams)

Page 7 of 8

Final Report of ASTM C 330-17a February 6, 2024

Bloated Material - Russell County Reclamation

SGS TEC Services Sample ID: 23-1479

Page 8 of 8

Total

Cycles

Completed

Fundamental

Transverse

Frequency, khz

Relative Dynamic

Modulus (%)

Weight Change

(grams)

Length Change

(inches)

Beam

1

Beam

2

Beam

3

Beam

1

Beam

2

Beam

3

Beam

1

Beam

2

Beam

3

Beam

1

Beam

2

Beam

3

0 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

36 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

72 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

108 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

144 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

180 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

216 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

252 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

288 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

300 1.731 1.731 1.731 100 100 100 0 0 0 0 0 0

Average Relative Dynamic Modulus 100 0 0

We appreciate the opportunity of providing our services to you. If you have any questions pertaining to

this report or need any additional information, please do not hesitate to call us.

Sincerely,

SGS, TEC SERVICES, INC.

Caleb Howard Steven Maloof

Project Manager Laboratory Principle/Sr. Project Manager

Final Report of ASTM C330-17a Bloated Material - Russell County Reclamation SGS TEC Services Sample ID: 23-1479

February 6, 2024

Fundamental . 5 a , Total Transverse Relative Dynamic Weight Change | Length Change Cycles Frequeney, khz Modulus (%) (grams) (inches) Completed [Beam ] Beam ] Beam | Beam] Beam ] Beam | Beam ] Beam | Beam | Beam | Beam | Beam 1 2 3 1f2f3faf2]3f1f2]s3 0 1731 [1.731 [1.731 | 100 | 100[ 100 f 0 f o [ 0 [ 0 | 0 | 0 36 1731 [1.731 [1.731 | 100 100[ 100 f 0 fo [ 0 [ 0 | 0 | 0 2 1731 [1.731 [1.731 | 100 100[ 100 f 0 fo [ 0 [ 0 | 0 | 0 108 1731 [1.731 [1.731 | 100 100[ 100 f 0 fo [ 0 [ 0 | 0 | 0 144 1731 [1.731 [1.731 | 100 100[ 100 f 0 fo [ 0 [ 0 | 0 | 0 180 1731 [1.731 [1.731 | 100 | 100; 100 f 0 fo [ 0 | 0 | 0 | 0 216 1731 [1.731 [1.731 | 100 | 100[ 100 f 0 fo [ 0 [ 0 | 0 | 0 252 1731 [1.731 [1.731 | 100 | 100[ 100 f 0 fo [ 0 [ 0 | 0 | 0 288 1731 [1.731 [1.731 | 100 | 100[ 100 f 0 fo [ 0 [ 0 | 0 | 0 300 1731 [1.731 [1.731 | 100 | 100; 100 f 0 fo [ 0 | 0 | 0 | 0 ‘Average Relative Dynamic Modulus 100 0 0

We appreciate the opportunity of providing our ser this report or need any additional information, please do not hesitate to call us.

Sincerely,

SGS, TEC SERVICES, INC.

ethene

Caleb Howard

Project Manager

Steven Maloof

es to you, If you have any questions pertaining to

Laboratory Principle/Sr. Project Manager

Page 8 of 8

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